forthcoming articles
The following articles are a selection of those recently accepted for publication in Journal of Synchrotron Radiation.
See also Forthcoming articles in all IUCr journals.
research papers
Signal-to-noise and spatial resolution in in-line imaging. 1. Basic theory, numerical simulations and planar experimental images
Signal-to-noise ratio and spatial resolution are quantitatively analysed in the context of propagation based X-ray phase-contrast imaging. We show that the performance of the method is determined by the Fresnel number and the ratio of the real decrement to the imaginary part of the refractive index of the imaged object.
letters to the editor
The HEPS Synchrotron unleashes new medical frontiers
The High Energy Photon Source (HEPS) in Beijing achieved a beam energy of 6GeV, positioning it as the world's brightest fourth-generation synchrotron with the smallest emittance. This milestone enables groundbreaking advances in health sciences and various research fields, promising new insights into biological and quantum processes.
research papers
Automated spectrometer alignment via machine learning
In this study, we showcase the application of a machine learning approach for the automated alignment of a soft X-ray spectrometer. Our method has been validated with experimental data at the beamline and significantly reduces the alignment time from approximately one hour to just a few minutes.
research papers
research papers
Development of a portable and cost-effective femtosecond fibre laser synchronizable with synchrotron X-ray pulses
This study introduces a compact, portable femtosecond fibre laser system optimized for synchronization with SPring-8 synchrotron X-ray pulses in a uniform filling mode, offering a practical and cost-effective alternative to traditional, fixedly installed laser systems for time-resolved spectroscopy combining synchrotron X-ray pulses and laser pulses.
research papers
Soft X-ray wavefront sensing at an ellipsoidal mirror shell
Phase retrieval at an axisymmetric ellipsoidal mirror is demonstrated with soft X-rays (277 eV), completed by a reconstruction of the focus as well as figure and alignment error of the mirror. Based on simple measurements of the cross-focal, three-dimensional intensity distribution, an intuitive algorithm is proposed which combines the advantages of high resolution, sensitivity, and reliability even under difficult conditions like a low source flux or weak spatial coherence.
research papers
feature articles
Investigation of fast and efficient lossless compression algorithms for macromolecular crystallography experiments
Many macromolecular crystallography beamlines are now fitted with DECTRIS Eiger detectors, which are all delivered with optimized compression algorithms by default; they perform well with current framing rates and typical diffraction data. However, better lossless compression algorithms have been developed and are now available to the research community.
research papers
Asymmetric electrostatic dodecapole: compact bandpass filter with low aberrations for momentum microscopy
A compact bandpass prefilter eliminates electrons with energies above or below the desired range and can correct image aberrations up to 3rd order before the beam enters a time-of-flight analyzer. We demonstrated the imaging performance of the filter for two key applications of the high-energy momentum microscope: full-field core-level photoelectron diffraction and mapping of bulk valence bands.
beamlines
High-throughput and high-resolution powder X-ray diffractometer consisting of six sets of 2D CdTe detectors with variable sample-to-detector distance and innovative automation system
A high-throughput and high-resolution powder X-ray diffractometer is developed at third experimental hutch of BL13XU, SPring-8. The diffractometer is equipped with six sets of 2D CdTe detectors and an automation system including sample exchange and equipment switching. The performance and demonstration results are presented.
research papers
Mapping of lithium ion concentrations in 3D structures through development of in situ correlative imaging of X-ray Compton scattering-computed tomography
A novel in situ correlative imaging X-ray Compton scattering computed tomography (XCS-CT) technique has been developed to unravel the fundamental relationship between the materials chemistry of light elements and their 3D structures. Here, this technique is applied to two types of batteries to map the internal lithium-ion concentrations.
research papers
research papers
research papers
In situ XAFS–XRD study of the Zr–Y2O3 interaction at extra-high temperatures
In situ XAFS–XRD measurements of Zr oxidation and the ZrO2–Y2O3 reaction up to 2519 K are reported. Analysis of anharmonic effects at high temperatures showed that Y2O3–ZrO2 proceeded to stabilize Zr—O and Y—O bonding. The developed system was confirmed to be applicable for high-temperature investigations of nuclear fuel material.
research papers
First X-ray spectral-ptychography and resonant ptychographic computed tomography experiments at the SWING beamline from Synchrotron SOLEIL
The first X-ray spectral ptychography and resonant ptychographic computed tomography experiments at the SWING beamline at Synchrotron SOLEIL are described. To illustrate the application of the techniques, a metallic Ni wire sample is measured.
short communications
Enhanced X-ray free-electron laser performance with optical klystron and helical undulators
This paper presents a demonstration of the improved performance of an X-ray free-electron laser using the optical klystron mechanism and helical undulator configuration, in comparison with the common planar undulator configuration without optical klystron. The measured improvements are compared with simulations and show a good agreement and a significant reduction in saturation length and an increase in saturation power.
research papers
research papers
Developing an in situ LED irradiation system for small-angle X-ray scattering at B21, Diamond Light Source
A system has been developed for irradiating samples with UV and visible light in situ during small-angle X-ray scattering data collection. The system is suitable for studying light-responsive samples such as photosurfactants, UV-hardening resins or light-active proteins.
research papers
The concept for hard X-ray beamline optics at SLS 2.0
A simple, easy-to-operate and robust beamline design is presented for five new hard X-ray beamlines in the scope of the latest upgrade of the Swiss Light Source. The performance increase is up to four orders of magnitude with respect to the current storage ring and beamline design.
teaching and education
Teaching about the birth of synchrotron light: the role of Frascati and a missed opportunity
A collection of personal reminiscences illuminates many widely unknown facts about the first steps of synchrotron radiation research; in particular, the events that brought Frascati close to world leadership in this domain.
research papers
research papers
Laminography as a tool for imaging large-size samples with high resolution
The laminography setup and software toolbox for efficient imaging of large-size samples are presented. Applicability of the developed technique is demonstrated by imaging slabs through a whole mouse brain sample stained with heavy elements.